ure to cool,
then pour it into a sep funnel. Wash the ethyl acetate solution with 50
ml of water to recover the lithium iodide into the water solution.
Separate off the water layer, and evaporate the water to recover the
lithium iodide for reuse. The ethyl acetate solution should be dried
over some anhydrous sodium sulfate, then the ethyl acetate evaporated
off to give about 20 grams of 2,4,5-trimethoxyphenlyacetone. This
light-sensitive substance should be stored in the freezer.
90
12 Studies On The Production OfTMA-2
91
Method Two
Acetonitrile is a quite poisonous solvent, dangerous both in
inhalation from the fizzing electrochemical cell and by absorption
through the skin. It has been my experience that just spilling a little bit of
it on your skin is enough to give you head rushes and make you feel
uncomfortable. The use of acetonitrile can be avoided without loss of
yield by using the alternative procedure in Example 6 in the patent.
The electrochemical cell is constructed in exactly the same way as in
the first method. Then into the electrochemical cell put 400 ml of
dimethylformamide, 200 ml of water containing 27 grams NaBr, and 20
grams asarone. Check the level of the solution, and make sure that the
amount of electrode surfaces are the same as in the first method. Then
begin stirring, and pass the current through the solution exactly as in the
first method.
When the 24,000 coulombs have been passed, pour the contents of
the beaker into a sep funnel, dilute with 1000 ml of a 20% solution of
salt in water, and extract four times with 200 ml portions of ethyl
acetate. The combined extracts, amounting to 800 ml, should be
washed twice with 200 ml portions of a 20% solution of salt in water.
The ethyl acetate solution contains the product epoxide. It should be
evaporated under a vacuum to a volume of about 200 ml, then reacted
with lithium iodide just as in the first method to yield about 20 grams of
2,4,5-trimethoxyphenylacetone.
Recycling of solvents is possible with this method too. Ethyl
acetate can be recovered during the vacuum evaporation by use of a
dry-ice trap. The dimethyl-formamide can be recovered by vacuum
distillation.
The Journal Method
A very effective alternative method exists for converting propenyl
benzenes to phenylacetones. I know through mail received from the
reading public that this method gives a yield of about 80% when used
Practical LSD Manufacture
92
with isosafrole. Similar results can be expected when used with
asarone.
In spite of the high yields and simplicity of this reaction, I can't
recommend its use. That's because this procedure uses thallium(III)
nitrate to oxidize the propenylbenzene to the corresponding
phenylacetone. The thallium(III) nitrate gets reduced to thallium(I)
nitrate. Both of these heavy-metal compounds are very poisonous and,
unlike organic chemicals, the heavy metals persist forever in the
environment, and accumulate in the body. You wa
Carl Epling, who first described S. divinorum, reported the newer as having a blue corolla, and it has been illustrated this way in the literature (Epling E Diet Diet Dieting and Jativa-M, 1962; Schultes, 1976). However, this description has been shown to be an error, as all living specimens of Can I Buy Ephedra the plant have had blossoms ephedra free with white corollas and purple calyces (Diaz, 1975a; Emboden, 1979).
Ephedra as weight loss supplement
Ephedra reduces appetite and stimulates fat metabolism, making it very effective as weight-loss supplement. The active compound in Ephedra (Ma Huang) is ephedrine. Ephedrine increases the metabolic rate, so that your body burns fats and sugar more efficiently. By mobilizing stored fat and carbohydrate reserves, ephedrine reduces your appetite.
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Some tips about losing weight with ephedra.
Ephedra, What Is This Herb? -Weight Loss Aid
Extended article on losing weight with ephedra, and effective combinations with other substances.
nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970).
To produce a one
ephedra ma huang
mole batch, dissolve one mole
Supercaps of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug.
In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol.
Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone
stacker by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
addition product.
12 Studies On The Production OfTMA-2
93
Production of TMA-2, MDA, etc. from the
Corresponding Phenylacetone
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948).
Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50
Raw Food Diet atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of
ephedra ma huang platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20
stackers
ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
to accomplish.
Back to Method 3 of Terrarium Construction.
table of contents.
Adaptation-20: Providing a Moisture Reservoir in the
Substrate
A reservoir for moisture can be built into the cake while packing the
jars with substrate material. Start with an empty jar and tamp 1/4 inch
of substrate material in the bottom. Next, position a magic marker or
some other object with a cylindrical shape and a diameter of about 3/4
inch in the center of the jar. Fill the jar as normal. Next, remove the
object and fill the bore with damp vermiculite. Lastly, pack 1/4 inch
of substrate material over the entire jar, sealing the damp vermiculite
inside the cake.
The damp vermiculite can be mixed separately from the substrate
material. Use about 1 cup of vermiculite and 1/3 cup of water. This
should produce enough damp vermiculite for a dozen 1/2 pint culture
jars.
After the cake has fruited, occasionally inject water into this
reservoir. The easiest place to inject is the position of the cake that
used to be at the center of the bottom of the jar. Just insert a syringe
filled with sterile water and inject water until it is full.
In case you are wondering, the substrate material can't be injected
with water directly. The rice flour and vermiculite form a very tight
seal and it is next to impossible to inject water. Even if you do
(30 of 39) 5/1/2002 6:54:26 PM]
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
manage to inject water, it doesn't spread through the cake. Having this
reservoir filled with damp vermiculite gives the mycelium network
access to a lot of moisture.
The easiest way we have found to implement this adaptation is to cut
the bottom off of a 10 cc syringe and press the bottom of the syringe
into the wet vermiculite several times. This will load the syringe with
wet vermiculite. Then place the syringe in the culture jar and pack the
substrate around it. Use the syringe's plunger to hold the wet
vermiculite stationary while you remove the syringe. Tamp an
additional 1/4 inch of substrate material over the entire surface of the
jar.
Advantage:
This adaptation will dramatically extend the longevity of the cake.
The cake's yield are normally limited by the amount of moisture in
the cake. This procedure allows you to replace moisture as it is
consumed by mushroom growth. In general, you will double the total
output of the cake compared to not implementing this adaptation.
Disadvantages:
It is a little bit of extra work to prepare the jars this way. Also, there is
a need to be careful to use sterile water when injecting moisture
during the growing phase. There is no way to check for contamination
introduced inside the cake by injecting water.
Back to preparation and colonization
table of contents.
Adaptation-21: Use of a Timer to Control Suspended Water
Droplets and Stimulate Fruiting
The ultra sonic humidifier can be placed on a timer to control the
amount of suspended water
Carl Epling, who first ephedra danger described S. divinorum, reported the newer as having a blue corolla, and it has been illustrated this way in the literature (Epling and Jativa-M, 1962; Schultes, 1976). However, this Prescription Diet Pill description has been shown to be an error, as all living specimens of Ephedra Based Product the plant have had blossoms with white corollas and purple calyces (Diaz, 1975a; Emboden, 1979).
ia
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Tyroplex™ (proprietary blend of l-tyrosine and acetyl-l-tyrosine), Green Tea Extract, Seropro™ (proprietary cocoa extract standardized for PEA (phenylethylamine), tyramine and theobromine), Yerba Mate, di-Methionine, Ginger Root, Isotherm™ (proprietary blend of quercetin and fisetin), Bitter Orange, DMAE (2-dimethylaminoethanol), Grape Seed Extract
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Metabolic Thyrolean
to accomplish.
Back to Method 3 of Terrarium Construction.
table of contents.
Adaptation-20: Providing a Moisture Reservoir in the
Substrate
A reservoir for moisture can be built into the cake while packing the
jars with substrate material. Start with an empty jar and tamp 1/4 inch
of substrate material in the bottom. Next, position a magic marker or
some other object with a cylindrical shape and a diameter of about 3/4
inch in the center of the jar. Fill the jar as normal. Next, remove the
object and fill the bore with damp vermiculite. Lastly, pack 1/4 inch
of substrate material over the entire jar, sealing the damp vermiculite
inside the cake.
The damp vermiculite can be mixed separately from the substrate
material. Use about 1 cup of vermiculite and 1/3 cup of water. This
should produce enough damp vermiculite for a dozen 1/2 pint culture
jars.
After the cake has fruited, occasionally inject water into this
reservoir. The easiest place to inject is the position of the cake that
used to be at the center of the bottom of the jar. Just insert a syringe
filled with sterile water and inject water until it is full.
In case you are wondering, the substrate material can't be injected
with water directly. The rice flour and vermiculite form a very tight
seal and it is next to impossible to inject water. Even if you do
(30 of 39) 5/1/2002 6:54:26 PM]
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
manage to inject water, it doesn't spread through the cake. Having this
reservoir filled with damp vermiculite gives the mycelium network
access to a lot of moisture.
The easiest way we have found to implement this adaptation is to cut
the bottom off of a 10 cc syringe and press the bottom of the syringe
into the wet vermiculite several times. This will load the syringe with
wet vermiculite. Then place the syringe in the culture jar and pack the
substrate around it. Use the syringe's plunger to hold the wet
vermiculite stationary while you remove the syringe. Tamp an
additional 1/4 inch of substrate material over the entire surface of the
jar.
Advantage:
This adaptation will dramatically extend the longevity of the cake.
The cake's yield are normally limited by the amount of moisture in
the cake. This procedure allows you to replace moisture as it is
consumed by mushroom growth. In general, you will double the total
output of the cake compared to not implementing this adaptation.
Disadvantages:
It is a little bit of extra work to prepare the jars this way. Also, there is
a need to be careful to use sterile water when injecting moisture
during the growing phase. There is no way to check for contamination
introduced inside the cake by injecting water.
Back to preparation and colonization
table of contents.
Adaptation-21: Use of a Timer to Control Suspended Water
Droplets and Stimulate Fruiting
The ultra sonic humidifier can be placed on a timer to control the
amount of suspended water
ephedra supercaps align="right"> 1 Grams
Digital Scales - Ephedra Fat UPTO 400 Gram / 0
ps from going in
the four holes in the lid while the jar is being sterilized. If you poked
your holes in the lid such that the sharp edges are pointing up, be
careful not to rip or puncture the tin foil. If you need to, you can add a
second or even a third piece of tin foil to make sure water will not drip
into the holes in the lid.
Step 8:
Now the culture jars need to be sterilized. Place the jars in a large
kitchen pot and add water so that water comes half way up the side of
the jars. Bring the water to a slow boil and place the lid on the pot.
From the time the water starts to boil, the jars need 1 hour to be
(4 of 29) 5/1/2002 6:54:17 PM]
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
sterilized.
Water should not be bubbling and splashing all over the
place. The jars should not be floating around in the water. The
substrate in the culture jars has the right amount of water in it already.
You do not want water leaking into the jars and changing the ratio.
The
jars should not sit flat on the bottom of the pan. Too much heat can
transfer directly to the jars and cause a loss of moisture. You can place
a wash cloth inside the pan and set the jars directly on the wash cloth
to help prevent too much heat from transferring to the jars.
Step 9:
Let the jars cool slowly.
Leave them covered in the pan that was used
to sterilize them. Let them cool completely. The jars need to be at or
close to room temperature in order to inoculate.
The spores will be
killed if the jars are not cool enough when they are inoculated. It will
take several hours to cool sufficiently. You may hear sounds as the jars
cool. This is normal.
Step 10:
Now comes the good part. Inoculation of the culture jars. Assuming
you have a viable, sterile spore syringe, you are now in a position to
inoculate the cultures and start the first phase of the growing cycle.
The needle of the spore syringe must be sterile. If your fingers or
anything other than the lid or contents of the culture jars comes in
contact with it, assume it is no longer sterile. If Detox Diet there is any doubt
about its condition, use a cigarette lighter to heat the entire needle.
Heat it until it glows red. Let it cool for a few minutes and squirt some
of the solution out of the syringe.
Shake the syringe. Make sure the spores are mixed well within the
syringe. This can be accomplished more easily if you pull the plunger
back on the syringe to get a little air into the syringe.
Remove the tin foil from each culture jar as you prepare to inoculate it.
Insert the needle of the syringe as far as it will go into a hole in the lid
of the culture jar and get the needle to press against the glass.
Examine
the next figure for a simple diagram of how things should look. Inject
1/4 cc of solution at a site under each hole in the lid. Adaptation-4 A
total of 1 cc of solution for each jar. Adaptation-5
(5 of 29) [5/1/2002 6:54:17 PM]
How To Grow Magic Mushrooms The ps from going in
the four holes in the lid while the jar is being sterilized.
If you poked
your holes in the lid such that the sharp edges are pointing up, be
careful not to rip or puncture the tin foil. If you need to, you can add a
second or even a third piece of tin foil to make sure water will not drip
into the holes in the lid.
Step 8:
Now the culture jars need to be sterilized. Place the jars in a large
kitchen pot and add water so that water comes half way up the side of
the jars. Bring the water to a slow boil and place the lid on the pot.
From the time the water starts to boil, the jars need 1 hour to be
(4 of 29) 5/1/2002 6:54:17 PM]
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
sterilized.
Water should not be bubbling and splashing all over the
place. The jars should not be floating around in the water. The
substrate in the culture jars has the right amount of water in it already.
You do not want water leaking into the jars and changing the ratio. The
jars should not sit flat on the bottom of the pan. Too much heat can
transfer directly to the jars and cause a loss of moisture. You can place
a wash cloth inside the pan and set the jars directly on the wash cloth
to help prevent too much heat from transferring to the jars.
Step 9:
Let the jars cool slowly.
Leave them covered in the pan that was used
to sterilize them. Let them cool completely. The jars need to be at or
close to room temperature in order to inoculate. The spores will be
killed if the jars are not cool enough when they are inoculated. It will
take several hours to cool sufficiently. You may hear sounds as the jars
cool. This is normal.
Step 10:
Now comes the good part. Inoculation of the culture jars. Assuming
you have a viable, sterile spore syringe, you are now in a position to
inoculate the cultures and start the first phase of the growing cycle.
The needle of the spore syringe must be sterile. If your fingers or
anything other than the lid or contents of the culture jars comes in
contact with it, assume it is no longer sterile. If there is any doubt
about its condition, use a cigarette lighter to heat the entire needle.
Heat it until it glows red. Let it cool for a few minutes and squirt some
of the solution out of the syringe.
Shake the syringe. Make sure the spores are mixed well within the
syringe. This can be accomplished more easily if you pull the plunger
back on the syringe to get a little air into the syringe.
Remove the tin foil from each culture jar as you prepare to inoculate it.
Insert the needle of the syringe as far as it will go into a hole in the lid
of the culture jar and get the needle to press against the glass.
Examine
the next figure for a simple diagram of how things should look. Inject
1/4 cc of solution at
stacker
a site under each hole in the lid. Adaptation-4 A
total of 1 cc of solution for each jar. Adaptation-5
(5 of 29) 5/1/2002 6:54:17 PM]
How To Grow Magic Mushrooms The ps from going in
the four holes in the lid while the jar is being sterilized. If you poked
your holes in the lid such that the sharp edges are pointing up, be
careful not to rip or puncture the tin foil. If you need to, you can add a
second or even a third piece of tin foil to make sure water will not drip
into the holes in the lid.
Step 8:
Now the culture jars need to be sterilized. Place the jars in a large
kitchen pot and add water so that water comes half way up the side of
the jars. Bring the water to a slow boil and place the lid on the pot.
From the time the water starts to boil, the jars need 1 hour to be
(4 of 29) [5/1/2002 6:54:17 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
sterilized.
Water should not be bubbling and splashing all over the
place. The jars should not be floating around in the water. The
substrate in the culture jars has the right amount of water in it already.
You do not want water leaking into the jars and changing the ratio. The
jars should not sit flat on the bottom of the pan. Too much heat can
transfer directly to the jars and cause a loss of moisture. You can place
a wash cloth inside the pan and set the jars directly on the wash cloth
to help prevent too much heat from transferring to the jars.
Step 9:
Let the jars cool slowly. Leave them covered in the pan that was used
to sterilize them. Let them cool completely. The jars need to be at or
close to room temperature in order to inoculate. The spores will be
killed if the jars are not cool enough when they are inoculated. It will
take several hours to cool sufficiently. You may hear sounds as the jars
cool. This is normal.
Step 10:
Now comes the good part. Inoculation of the culture jars. Assuming
you have a viable, sterile spore syringe, you are now in a position to
inoculate the cultures and start the first phase of the growing cycle.
The needle of the spore syringe must be sterile. If your fingers or
anything other than the lid or contents of the culture jars comes in
contact with it, assume it is no longer sterile. If there is any doubt
about its condition, use a cigarette lighter to heat the entire needle.
Heat it until it glows red. Let it cool for a few minutes and squirt some
of the solution out of the syringe.
Shake the syringe. Make sure the spores are mixed well within the
syringe. This can be accomplished more easily if you pull the plunger
back on the syringe to get a little air into the syringe.
Remove the tin foil from each culture jar as you prepare to inoculate it.
Insert the needle of the syringe as far as it will go into a hole in the lid
of the culture jar and get the needle to press against the glass. Examine
the next figure for a simple diagram of how things should look. Inject
1/4 cc of solution at a site under each hole in the lid. Adaptation-4 A
total of 1 cc of solution for each jar. Adaptation-5
(5 of 29) [5/1/2002 6:54:17 PM
How To Grow Magic Mushrooms The ps from going in
the four holes in the lid while the jar is being sterilized. If you poked
your holes in the lid such that the sharp edges are pointing up, be
careful not to rip or puncture the tin foil. If you need to, you can add a
second or even a third piece of tin foil to make sure water will not drip
into the holes in the lid.
Step 8:
Now the culture jars need to be sterilized. Place the jars in a large
kitchen pot and add water so that water comes half way up the side of
the jars. Bring the water to a slow boil and place the lid on the pot.
From the time the water starts to boil, the jars need 1 hour to be
(4 of 29) 5/1/2002 6:54:17 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
sterilized. Water should not be bubbling and splashing all over the
place. The jars should not be floating around in the water. The
substrate in the culture jars has the right amount of water in
metabolife with ephedra it already.
You do not want water leaking into the jars and changing the ratio. The
jars should not sit flat on the bottom of the pan. Too much heat can
transfer directly to the jars and cause a loss of moisture. You can place
a wash cloth inside the pan and set the jars directly on the wash cloth
to help prevent too much heat from transferring to the jars.
Step 9:
Let the jars cool slowly.
Leave them covered in the pan that was used
to sterilize them. Let them cool completely. The jars need to be at or
close to room temperature in order to inoculate. The spores will be
killed if the jars are not cool enough when they are inoculated. It will
take several hours to cool sufficiently. You may hear sounds as the jars
cool. This is normal.
Step 10:
Now comes the good part. Inoculation of the culture jars. Assuming
you have a viable, sterile spore syringe, you are now in a position to
inoculate the cultures and start the first phase of the growing cycle.
The needle of the spore syringe must be sterile. If your fingers or
anything other than the lid or contents of the culture jars comes in
contact with it, assume it is no longer sterile. If there is any doubt
about its condition, use a cigarette lighter to heat the entire needle.
Heat it until it
Lipodrene Side Effects Hallucinations Ephedrine Plus glows red. Let it cool for a few minutes and squirt some
of the solution out of the syringe.
Shake the syringe. Make sure the spores are mixed well within the
syringe. This can be accomplished more easily if you pull the plunger
back on the syringe to get a little air into the syringe.
Remove the tin foil from each culture jar as you prepare to inoculate it.
Insert the needle of the syringe as far as it will go into a hole in the lid
of the culture jar and get the needle to press against the glass. Examine
the next figure for a simple diagram of how things should look. Inject
1/4 cc of solution at a site under each hole in the lid. Adaptation-4 A
total of 1 cc of solution for each jar. Adaptation-5
(5 of 29) 5/1/2002 6:54:17 PM
How To Grow Magic Mushrooms The nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
addition product.
12 Studies On The Production OfTMA-2
93
Production of TMA-2, MDA, etc. from the
Corresponding Phenylacetone
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
Carl Epling, who first described S. divinorum, reported the newer as having a blue
Diet Forum Diet corolla, and it has been illustrated this way in the literature (Epling and Jativa-M, 1962; Schultes, 1976). However, this description has been shown to be an error, as all living specimens of the plant have had blossoms with white corollas and purple calyces (Diaz,
product containing ephedra
1975a; Emboden, 1979).
Yohimbe is a tree that grows throughout the African nations of Cameroon, Gabon and Zaire. (A similar plant in South America is called Quebracho). For centuries, natives from these areas have ingested both the crude bark and purified compound as a tonic to enhance sexual prowess and as an aphrodisiac. The bark has been smoked as a hallucinogen and has been used in traditional medicine to treat angina and hypertension. The herb is a sensual stimulant for healthy men and women. Today, doctors prescribe an extract from the tree to treat organic impotence.
Yohimbe's energizing effects stem from it's ability to increase blood flow to the genitals, both male and female. It is thought to stimulate the pelvic nerve ganglia and thus is helpful for men with erection problems. In fact a prescription drug, yohimbine hydrochloride, is the only FDA approved drug for impotence. Effects can include increased libido, increased sensation and increased stamina. Women have also reported similar effects and general pleasant sensations.
Yohimbe bark contains about 6% yohimbine. This constituent is an indole alkaloid that is classified as an alpha-2-adrenergic blocking agent. The herb has a general nervous system stimulatory effect and can cause changes in blood pressure by dilating blood vessels. It can increase the heart rate, raise body temperature and increase blood pressure. At higher dosages, it has a mild psychotropic effect.
Yohimbe bark stimulates chemical reactions in the body that may aid in psychogenic cases of impotence, due to fatigue, tension and stress. Clinical studies have shown the herb to be effective in restoring potency in diabetic and heart patients who suffer from impotency. As an alpha-adrenoreceptor blocker, yohimbe reduces the effect of hormones that cause constriction of blood vessels, which typically increases as we age. It increases the body's production of norepinephrine which is essential in the formation of erections. Yohimbe may also boost the adrenaline supply to nerve endings, which can quicken male sensual stimulation. It has been used in combination with ginseng and saw palmetto as a remedy for men with low sex drive.
Yohimbe is also a short term MAO (monoamine oxidase) inhibitor and should be used with caution, especially if you have high blood pressure. Being an MAO inhibitor, yohimbe should not be taken with any food or drink containing tyramines (cheese, chocolate, beer, aged meats, nuts, etc.) and particularly not with the amino acids tyrosine or phenylalanine. A rise in blood pressure can result from the body not being able to remove the tyramines from these foods. It may be dangerous if used with anti-depressants, sedatives, antihistamines, caffeine, or amphetamines. Yohimbe may have other side effects such as racing heart rate, irritability, headache, nausea, sweating, dizziness and frequent urination. Anyone with a heart condition, kidney disease, glaucoma or history of gastric or duodenal ulcers should avoid
nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method Can I Buy Ephedra is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product.
One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Hallucinogenic Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
addition product.
12 Studies On The Production OfTMA-2
93
Production of TMA-2, MDA, etc. from the
Corresponding Phenylacetone
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about ephedra side effects 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
Amongst the Mazatecs, Salvia divinorum (Diviner's sage) is known under such names as ska Maria Pastora and Hierba Maria, which translate as "the herb of Mary" or "leaves of Mary the Shepherdess". In a recent paper, Jonathan 0tt has noted that the Mazatecs lack an indigenous name for Salvia divinorum, both the Christian theme of Mary, as well as sheep, having been introduced to the region during the Spanish conquest. The Mazatecs also list a method of consuming this plant that does not efficiently utilize its psychoactive content, and seem to be generally unaware of its tremendous potency. Based on this information, and the likelihood of its being a cultigen, Ott has suggested that Salvia divinorum may be a post-conquest introduction to the Sierra Mazateca. However, it has also been suggested, initially by R. Gordon Wasson, that Salvia divinorum may be the Aztec plant Pipiltzintzintli, an entheogen that was briefly described by a 17th century Spanish friar. Ott has found that the little information available regarding Pipiltzintzintli supports this hypothesis, while ruling out several other plants that have been suggested as candidates for this Aztec sacrament.
ure to cool,
then pour it into a sep funnel. Wash the ethyl acetate solution with 50
ml of Ecstasy water to recover the lithium iodide into the water solution.
Separate off the water layer, and evaporate the water to recover the
lithium iodide for reuse. The ethyl acetate solution should be dried
over some anhydrous sodium sulfate, then the ethyl acetate evaporated
off to give about 20 grams of 2,4,5-trimethoxyphenlyacetone. This
light-sensitive substance should be stored in the freezer.
90
12 Studies On The Production OfTMA-2
91
Method Two
Acetonitrile is a quite poisonous solvent, dangerous both in
inhalation from the fizzing electrochemical cell and by absorption
through the skin. It has been my experience that just spilling a little bit of
it on your skin is enough to give you head rushes and make you feel
uncomfortable. The use of acetonitrile can be avoided without loss of
yield by using the alternative procedure in Example 6 in the patent.
The electrochemical cell is constructed in exactly the same way as in
the first method. Then into the electrochemical cell put 400 ml of
dimethylformamide, 200 ml of water containing 27 grams NaBr, and 20
grams asarone. Check the level of the solution, and make sure that the
amount of electrode surfaces are the same as in the first method. Then
begin stirring, and pass the current through the solution exactly as in the
first method.
When the 24,000 coulombs have been passed, pour the contents of
the beaker into a sep funnel, dilute with 1000 ml of a 20% solution of
salt in water, and extract four times with 200 ml portions of ethyl
acetate. The combined extracts, amounting to 800 ml, should be
washed twice with 200 ml portions of a 20% solution of salt in water.
The ethyl acetate solution contains the product epoxide. It should be
evaporated under a vacuum to a volume of about 200 ml, then reacted
with lithium iodide just as in the first method to yield about 20 grams of
2,4,5-trimethoxyphenylacetone.
Recycling of solvents is possible with this method too. Ethyl
acetate can be recovered during the vacuum evaporation by use of a
dry-ice trap. The dimethyl-formamide can be recovered by vacuum
distillation.
The Journal Method
A very effective alternative method exists for converting propenyl
benzenes to phenylacetones.
I know through mail received from the
reading public that this method gives a yield of about 80% when used
Practical LSD Manufacture
92
with isosafrole. Similar results can be expected when used with
asarone.
In spite of the high yields and simplicity of this reaction, I can't
recommend its use. That's because this procedure uses thallium(III)
nitrate to oxidize the propenylbenzene to the corresponding
phenylacetone. The thallium(III) nitrate gets reduced to thallium(I)
nitrate. Both of these heavy-metal compounds are very poisonous and,
unlike organic chemicals, the heavy metals persist forever in the
environment, and accumulate in the body. You wa
Yohimbe is a tree that grows throughout the African nations of Cameroon,
Can I Buy Ephedra Gabon and Zaire. (A similar plant in South America is called Quebracho). For centuries, natives from these areas have ingested both the crude bark and purified compound as a tonic to enhance sexual prowess and as an aphrodisiac. The bark has been smoked as a hallucinogen and has been used in traditional medicine to treat angina and hypertension. The herb is a sensual stimulant for healthy men and women. Today, doctors prescribe an extract from the tree to treat organic impotence.
Yohimbe's energizing effects stem from it's ability to increase blood flow to the genitals, both male and female. It is thought to stimulate the pelvic nerve ganglia and thus is helpful for men with erection problems. In fact a prescription drug, yohimbine hydrochloride, is the only FDA approved drug for impotence. Effects can include increased libido, increased sensation and increased stamina.
Women have also reported similar effects and general pleasant sensations.
Yohimbe bark contains about 6% yohimbine. This constituent is an indole alkaloid that is classified as an alpha-2-adrenergic blocking agent.
The herb has a general nervous system stimulatory effect and can cause changes in blood pressure by dilating blood
ephedra product
vessels. It can increase the heart rate, raise body temperature and increase blood pressure. At higher dosages, it has a mild psychotropic effect.
Yohimbe bark stimulates chemical reactions in the body that may aid in psychogenic cases of impotence, due to fatigue, tension
1200 Calorie Diet and stress. Clinical studies have shown the herb to be effective in restoring potency in diabetic and heart patients who suffer from impotency. As an alpha-adrenoreceptor blocker, yohimbe reduces the effect of hormones that cause constriction of blood vessels, which typically increases as we age. It increases the body's production of norepinephrine which is essential in the formation of erections.
Yohimbe may also boost the adrenaline supply to nerve endings, which can quicken male sensual stimulation.
It has been used in combination with ginseng and saw palmetto as a remedy for men with low sex drive.
Yohimbe is also a short term MAO (monoamine oxidase) inhibitor and should be used with caution, especially if you have high blood pressure. Being an MAO inhibitor, yohimbe should not be taken with any food or drink containing tyramines (cheese, chocolate, beer, aged meats, nuts, etc.) and particularly not with the amino acids tyrosine or phenylalanine. A rise in blood pressure can result from the body not being able to remove the tyramines from these foods. It may be dangerous if used with anti-depressants, sedatives, antihistamines, caffeine, or amphetamines.
Yohimbe may have other side effects such as racing heart rate, irritability, headache, nausea, sweating, dizziness and frequent urination. Anyone with a heart condition, kidney disease, glaucoma or history of gastric or duodenal ulcers should avoid
Ephedra as a 'smart' drug and energizer
Ephedra or Ma Huang contains the active compound ephedrine. Ephedrine stimulates the central nervous system and provides energy and increases alertness. A higher dose ephedra gives a nice tingling sensation over the head but also on the rest of your body. Ephedra acts a bit like XTC, only milder in its action and less speedy. Ephedra does give the same emphatic feeling as XTC does.
Ephedra and sex
The emphatic feelings and the energy makes ephedra suitable as love enhancer. Although some people claim they get to nervous and restless. So you should test this for yourself.
How to use Ephedra
The best way to take ephedra is in a capsule, but you can also make tea of the ephedra (ma huang) herb. After a certain point taking a higher dose ephedra does not intensify the trip, only taking cafein or guarana might help then. A single dose Ephedra is effective for 6 to10 hours. In the articles below you can find more information on how ephedra works as energizer.
Ephedra
General information about the qualities of ephedra from the Herbal Information Center.
Ephedrine As Amphetamine And Party-drug
Informative article on how ephedra can be an alternative for chemical party-drugs.
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Ephedra (also known as Ma huang, Chinese Ephedra and epitonin) is the worlds oldest medicine. The Chinese discovered ephedra more than 5000 years ago. Research has shown that ephedra increases metabolism and helps promote weight loss, relaxes the air passages in the lungs to help treat asthma and cough, promotes perspiration to help a person recover from a minor cold and helps promote urination to help relieve edema.
Ephedra has been widely researched for its thermogenic (fat burning) properties. Research has show that ephedra helps promote the loss of fat while helping spare lean muscle tissue, a highly sought-after property that prescription diet medications still have not been able to reproduce.
Herbal Phen-Fen, a popular herbal formulation used f
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